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具有初始孔隙的速溶咖啡冷凍干燥試驗
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國家自然科學基金項目(21676042)和遼寧省自然科學基金項目(201602167)


Experiment on Freeze-drying of Instant Coffee with Initial Porosity
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    摘要:

    為了縮短冷凍干燥時間,,降低過程能耗,研究了初始非飽和物料干燥技術在速溶咖啡的冷凍干燥工藝中的應用,。以速溶咖啡為溶質,,制備了具有不同初始飽和度的冷凍咖啡物料樣品,,并進行了冷凍干燥試驗,。研究結果表明,,相對于傳統(tǒng)的咖啡冷凍干燥,,初始非飽和咖啡物料能夠顯著強化冷凍干燥過程,。干燥產品SEM形貌顯示,,初始非飽和物料的干燥產品具有疏松的球狀孔隙空間,孔隙之間連通性好,,有利于水蒸氣的遷移,。在干燥室壓力11~33Pa條件下,壓力對冷凍干燥過程幾乎沒有影響,,提高環(huán)境溫度有利于縮短冷凍干燥時間,,組合加熱能夠進一步強化冷凍干燥過程。當溫度超過45℃時,,飽和物料會發(fā)生崩塌,,而非飽和物料則能夠保持穩(wěn)定的結構。飽和咖啡物料的冷凍干燥過程經歷升速,、恒速和降速3個階段,,非飽和物料則始終處于降速階段。

    Abstract:

    In order to decrease the freeze-drying time and reduce the process energy consumption, frozen coffee materials with prefabricated porosity were prepared and freeze-dried to explore its influence on freeze-drying experimentally. Instant coffee was selected as the solute in aqueous solution. Results showed that freeze-drying can be remarkably enhanced with the initially unsaturated frozen material compared with the traditionally saturated one. SEM images of dried products revealed that the initial unsaturated material had the spherical and uniformed porous structure, which was favorable to migration of sublimated vapor and improvement of the drying rate. Chamber pressure, which was ranged from 11Pa to 33Pa, had little effect on the freeze-drying process and increasing ambient temperature can be beneficial to the freeze-drying process. Combined heating can significantly reduce the drying time further. When the temperature was above 45℃, the saturated material was found to collapse causing the failure of freeze-drying. In contrast, the unsaturated one can bear higher operation temperature resulting in a relatively high drying efficiency. The conventionally saturated material experiences the raising rate stage, constant rate stage and falling rate stage during freeze-drying, while the unsaturated material was always in the falling rate stage throughout the process. Freeze-drying of initially unsaturated material would impose significant effect on the traditional freeze-drying process of agricultural products.

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王維,李強強,陳國華,李恒樂,楊菁,張朔.具有初始孔隙的速溶咖啡冷凍干燥試驗[J].農業(yè)機械學報,2018,49(6):347-353. WANG Wei, LI Qiangqiang, CHEN Guohua, LI Hengle, YANG Jing, ZHANG Shuo. Experiment on Freeze-drying of Instant Coffee with Initial Porosity[J]. Transactions of the Chinese Society for Agricultural Machinery,2018,49(6):347-353.

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  • 收稿日期:2018-02-08
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  • 在線發(fā)布日期: 2018-06-10
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