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水酶法制取大豆油乳狀液射流空化破乳工藝優(yōu)化
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國(guó)家重點(diǎn)研發(fā)計(jì)劃項(xiàng)目( 2016YFD0401402),、黑龍江省應(yīng)用技術(shù)研究與開(kāi)發(fā)計(jì)劃重大項(xiàng)目(GA17B002),、黑龍江省博士后面上資助經(jīng)費(fèi)項(xiàng)目(LBH-Z18030)和黑龍江省自然科學(xué)基金項(xiàng)目(C2018024)


Optimization of Emulsion Demulsification Technique with Jet Cavitation for Water-enzymatic Soybean Oil
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    摘要:

    為探究射流空化對(duì)水酶法制取大豆油所產(chǎn)生乳狀液的破乳機(jī)制,,通過(guò)光散射粒徑,、破乳率,、總提油率和乳狀液顯微結(jié)構(gòu)為指標(biāo)分別考察射流空化壓力、射流空化溫度和射流空化時(shí)間對(duì)乳狀液破乳機(jī)制的影響,。破乳率和總提油率隨著射流空化壓力(0.2~1.0MPa),、射流空化溫度(80~120℃)、射流空化時(shí)間(5~25s)的增加而增加,,射流空化作用實(shí)現(xiàn)徹底破乳后,,破乳率和總提油率反而下降。乳狀液粒徑分布及激光共聚焦顯微鏡顯示破乳后分散的小粒徑油滴轉(zhuǎn)變成直徑較大的油滴,。在單因素試驗(yàn)基礎(chǔ)上,,采用響應(yīng)面分析法對(duì)射流空化輔助水解破乳工藝條件進(jìn)行優(yōu)化,確定最優(yōu)破乳工藝條件為:射流空化壓力0.8MPa,、射流空化溫度100.92℃,、射流空化時(shí)間21.38s,此條件下破乳率為90.29%,,總提油率為87.06%,。

    Abstract:

    In order to explore the demulsification mechanism of soybean oil emulsion produced by aqueous enzymatic method, the effects of jet cavitation pressure, jet cavitation temperature and jet cavitation time on the demulsification mechanism of soybean oil emulsion were investigated by light scattering particle size analysis, demulsification rate, total oil extraction rate and emulsion microstructure. The results showed that the demulsification rate and total oil extraction rate were increased with the increase of jet cavitation pressure (0.2~1.0MPa), jet cavitation temperature (80~120℃) and jet cavitation time (5~25s). After the complete demulsification, the demulsification rate and total oil extraction rate were decreased. The particle size distribution of emulsion and laser confocal microscopy showed that the dispersed small size oil droplets were changed into larger diameter oil droplets after demulsification. On the basis of single factor experiment, response surface methodology was used to optimize the process conditions of jet cavitation assisted hydrolysis demulsification. The optimum demulsification conditions were determined as follows: jet cavitation pressure was 0.8MPa, jet cavitation temperature was 100.92℃, jet cavitation time was 21.38s. Under this condition, the demulsification rate was 90.29%, and the total oil extraction rate was 87.06%. The research result provided a theoretical basis for jet cavitation assisted enzymatic demulsification technology, and it was beneficial to the industrial application and promotion of aqueous enzymatic oil extraction technology.

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李良,田甜,吳長(zhǎng)玲,李楊,江連洲,王中江.水酶法制取大豆油乳狀液射流空化破乳工藝優(yōu)化[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2019,50(9):357-363. LI Liang, TIAN Tian, WU Changling, LI Yang, JIANG Lianzhou, WANG Zhongjiang. Optimization of Emulsion Demulsification Technique with Jet Cavitation for Water-enzymatic Soybean Oil[J]. Transactions of the Chinese Society for Agricultural Machinery,2019,50(9):357-363.

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  • 收稿日期:2019-03-01
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  • 在線發(fā)布日期: 2019-09-10
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